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1416134-48-9

  • Product NameAvibactam INT 1
  • Molecular FormulaC17H24N2O7
  • Molecular Weight368.387
  • Purity99%
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Product Details

Quick Details

  • CasNo： 1416134-48-9
  • Molecular Formula： C17H24N2O7
  • Purity： 99%

Reputable Factory Supply Top Purity Avibactam INT 1 1416134-48-9 with the Best Price

  • Molecular Formula:C15H22N2O3.C2H2O4
  • Molecular Weight:368.387
  • PSA：134.19000 
  • LogP:1.26680 

1416134-48-9 Relevant articles

Method for synthesizing avibactam intermediate compound

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Paragraph 0040; 0041; 0047; 0048; 0050; 0051; 0057-0059, (2019/11/20)

The invention relates to a method for sy...

A method of recovering and utilizing avibactam intermediate production waste liquid

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Paragraph 0052-0054, (2018/03/01)

The invention relates to a method of rec...

PROCESSES FOR PREPARING HETEROCYCLIC COMPOUNDS INCLUDING TRANS-7-OXO-6-(SULPHOOXY)-1,6-DIAZABICYCLO[3,2,1]OCTANE-2-CARBOXAMIDE AND SALTS THEREOF

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Page/Page column 17, (2013/02/27)

The present invention relates to compoun...

1416134-48-9 Process route

5-benzyloxyiminopiperidine-2S-carboxylic acid ethyl ester
1416134-60-5

5-benzyloxyiminopiperidine-2S-carboxylic acid ethyl ester

oxalic acid
144-62-7,97993-78-7

oxalic acid

ethyl (2S,5R)-5-[(benzyloxy)amino]piperidine-2-carboxylate oxalic acid salt
1416134-48-9

ethyl (2S,5R)-5-[(benzyloxy)amino]piperidine-2-carboxylate oxalic acid salt

Conditions
Conditions Yield
5-benzyloxyiminopiperidine-2S-carboxylic acid ethyl ester; With sulfuric acid; In ethyl acetate; at -20 - -15 ℃; for 1h;
With sodium tris(acetoxy)borohydride; In ethyl acetate; at -20 - -15 ℃; for 5h;
oxalic acid; In methanol; ethyl acetate; at 45 ℃; for 2h;
65.4%
5-benzyloxyiminopiperidine-2S-carboxylic acid ethyl ester; With sodium tetrahydroborate; sulfuric acid; propionic acid; In ethyl acetate; at -20 ℃;
With ammonia; In water; ethyl acetate;
oxalic acid; In ethanol; at 40 - 45 ℃;
 
ethanol
64-17-5

ethanol

(2S,5R)-5-benzyloxyaminopiperidin-2-carboxylic acid benzyl ester oxalic acid salt
1171080-45-7,1416134-44-5

(2S,5R)-5-benzyloxyaminopiperidin-2-carboxylic acid benzyl ester oxalic acid salt

sodium ethanolate
141-52-6

sodium ethanolate

oxalic acid
144-62-7,97993-78-7

oxalic acid

ethyl (2S,5R)-5-[(benzyloxy)amino]piperidine-2-carboxylate oxalic acid salt
1416134-48-9

ethyl (2S,5R)-5-[(benzyloxy)amino]piperidine-2-carboxylate oxalic acid salt

Conditions
Conditions Yield
ethanol; (2S,5R)-5-benzyloxyaminopiperidin-2-carboxylic acid benzyl ester oxalic acid salt; sodium ethanolate; at 0 ℃; for 1h;
oxalic acid; In ethyl acetate; acetone; at 35 ℃;
94%

1416134-48-9 Upstream products

  • 64-17-5
    64-17-5

    ethanol

  • 1171080-45-7
    1171080-45-7

    (2S,5R)-5-benzyloxyaminopiperidin-2-carboxylic acid benzyl ester oxalic acid salt

  • 141-52-6
    141-52-6

    sodium ethanolate

  • 144-62-7
    144-62-7

    oxalic acid

1416134-48-9 Downstream products

  • 1192491-61-4
    1192491-61-4

    (2S,5R)-1,6-diazabicyclo[3.2.1]octane-2-carboxamide 7-oxo-6-(sulfoxy)monosodium salt

  • 1192651-80-1
    1192651-80-1

    ({[(2S,5R)-2-carbamoyl-7-oxo-6-(sulfooxy)-1,6-diazabicyclo[3,2,1]-oct-6-yl]oxy}sulfonyl)tetrabutylammonium salt

  • 1416134-63-8
    1416134-63-8

    (2S,5R)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octan-2-carboxylic acid ethyl ester

  • 1192500-31-4
    1192500-31-4

    (2S,5R)-2-carbamoyl-7-oxo-1,6-diazabicylco[3.2.1]octan-6-yl hydrogensulfate

;

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